Organic Preparations and Procedures International
The New Journal for Organic Synthesis


Table of Contents Volume 25, 1993

Synthetic Applications of Diaryl Ether Photochemistry. A Review by R. Pollard and P. Wan*1
Chemistry of N-Methoxy-N-methylamides. Applications in Synthesis.A Review by M. P. Sibi15
Homoenolates and Other Functionalized Organometallics. A Review by M. T. Crimmins* and P. G. Nantermet43
The Reactions of some Alkoxycarbonyl Isothiocyanates with Alcohols, Phenols and Amines by A. R. Katritzky*, M. K. Bernard, Q. Long, L. Xie, N. Malhotra and M. Beltzer83
A Simple Synthesis of 1-Hydroxyalkyl-1,2,3,4-tetrahydroisoquinolines by L. Lázár, F. Fülöp, G. Bernáth* and J. Mattinen91
OPPI Briefs (J.-P. Anselme, Editor)99
Acetylation of 4-Amino-4,5-dihydro-1H-1,2,4-triazol-5-ones by A. A. Ikizler* and H. Yüksek99
Synthesis of Some Benzothiazolobenzotriazepinesby M. V. Deshmukh and D. S. Deshpande*105
A New Route for the Synthesis of Z-11-Hexadecen-1-ol, a Sex Pheromone of Chilo Infuscatellus (SNELL) by S. Narasimhan* and K. Ganeshwarprasad108
Synthesis of C-24 Thiazolidinone and Oxazolidinone Derivatives of Bile Acids by A. U. Siddiqui*, A. H. Siddiqui and T. S. Ramaiah110
An Improved Synthetic Route to Trifluoromethyl-6-substituted-2(1H)-pyridones by B. Narsaiah, A. Sivaprasad and R. V. Venkataratnam*116
A Convenient One-Pot Synthesis of Novel Functionalized Terphenyls by V. V. Suresh and H. M. Chawla*118
A Convenient Synthesis of 2-Aminoalkyl Allyl Ethers by A. Dobrev122
Preparation of Low Molecular Weight, Optically Active Allylic Alcohols from (S)-(-)-Ethyl Lactate by J. C. McKew and M. J. Kurth*125
An Improved Preparation of 2,4-Dinitrophenyl Thioethers from Thiolcarbonic Esters by K. Harano, M. Eto, S. Kubota and T. Hisano*130
A Convenient Preparation of N-Demethyldiltiazem and its Conversion to a Diltiazem Homolog by J. Alexander133
The One-step Synthesis of p-tert-Butylcalix[5]arene by D. R. Stewart and C. D. Gutsche*137
The Use of Isocyanides in Heterocyclic Synthesis. A Review by S. Marcaccini and T. Torroba*141
An Efficient, Large-scale Synthesis of Triisopentadecanoin by T. A. Foglia* and P. D. Vail209
Selenium Oxide Oxidation of Abieta-7,13-dienes in Methanol by A. San Feliciano*, J. M. M. del Corral, M. Gordaliza and M. A. Salinero215
Convenient Synthesis of 6-Methyl, 8-Methyl and 6,8-Dimethyl Derivatives of 5-Hydroxy-1,2,3,4-tetrahydro-2-quinolinone by D. Blondet*, F. Laure and J.-C. Pascal223
OPPI Briefs (J.-P. Anselme, Editor)229
Improved Preparation of Aminomethylenemalonic Acid Derivatives by Tin-Promoted Addition of Diethyl Malonates to Nitriles by M. Nicolini* and A. Citterio229
Improved and Convenient Synthesis of Disulfides in the Absence of Solvent Catalyzed by Clayfen by H. M. Meshram232
Synthesis of 2-Dimethylamino-5-(α-Chloroalkenyl)-1,3-oxazin-6-ones by E. M. Beccalli* and A. Marchesini234
The Synthesis of Two Bicyclo[4.3.0]nonane Derivatives by C. W. Bird* and R. Cooper237
Michael Reaction of Fluorene and Indene by Phase-Transfer Catalysis by Y. Chaoguo*, L. Wenxing and W. Jitao241
Preparation of the Racemate and Enantiomers of 3-Hydroxy-5,5-dimethylhexanoic Acid by W. J. Brouillette*, A. S. Abuelyaman, C. A. Hosmer, R. N. Comber and A. Saeed243
An Efficient Preparation of 2H-[5,4-b]-Pyridoisothiazolone by S. W. Wright* and R. L. Corbett247
An Improved Synthesis of 1-(t-Butyloxycarbonyl)-3-(bromomethyl)indole by T. K. Venkatachalam, S. Mzengeza and M. Diksic*249
Synthesis of 3,6-Dimethoxy-2-naphthaldehyde by A. M. Moussa*, J.-R. Yang and M. E. Langmuir252
A Practical Procedure for the Synthesis of 5-substitued γ-Lactams by Z. Y. Wei and E. E. Knaus*255
Synthesis of Carcinogenic Benz[c]acridines. A Review by N. Motohashi*, J. Emrani, R. Meyer and M. Kawase259
Synthesis of New Substituted Pyridazines by A. H. H. Elghandour*, M. K. A. Ibrahim, I. S. A. Hafiz and M. H. Elnagdi293
Synthesis of Heterocyclic Compounds of Potential Biological Activity via the Stobbe Condensation by V. B. Baghos, S. H. Doss* and E. F. Eskander301
Macrocycle Syntheses: Cyclic Ketones, Ketoalkenes, Diketones and Dienes of Ring Size C21 to C26 by M. D. E. Forbes* and Y. Dang309
1,1'-Carbonyldibenzotriazole and 1,1'-Sulfonyldibenzotriazole. Versatile Reagents for the Dehydration of Aldoximes and Amides to Nitriles by A. R. Katritzky*, G.-F. Zhang and E.-Q. Fan315
Enantioselective Synthesis of (4R)-4-Nonanolide and (5R)-5-Decanolide from a Common Intermediate by H. R. Mohan and A. S. Rao*321
OPPI Briefs (J.-P. Anselme, Editor)327
Reaction of Pivaloylacetonitrile with Aromatic Aldehydes by K. Popandova-Yambolieva* and T. Iossifova327
A Convenient Synthesis of (±)-10-Methyl-2-tridecanone. The Pheromone of Southern Corn Rootworm by A. Sharma, A. Pawar, S. Chattopadhyay and V. R. Mamdapur*330
A Short Synthesis of (11Z,15Z)-Eicosadienoic Acid. A Compound of Marine Sponge Origin by B. A. Kulkarni, A. Chattopadhyay and V. R. Mamdapur*333
Convenient Synthesis of 2-Phenethyl Alcohol by Hydrolysis of 2-Bromoethylbenzene Under Phase-Transfer Conditions by H. A. Zahalka* and Y. Sasson336
Improvement of the Vilsmeier-Haack Reaction by D. Blaser, M. Calmes, J. Daunis*, F. Natt, A. Tardy-Delassus and R. Jacquier338
Synthesis of 2-Hydroxy-3-methylcyclopent-2-en-1-one from Linalyl Acetate by M. L. dos Santos and G. C. de Magalhães*341
A Simple Synthesis of Brassilexin, a Cruciferae Phytoalexin by M. Devys and M. Barbier*344
Vilsmeier Reaction of 3-Methyl-N-(4'-substituted)-azobenzenesulfonamido-2-quinoxalinone Dyes by I. M. A. Awad347
New Chemical Conversions of 5-Hydroxymethylfurfural and the Electrochemical Oxidation of its Derivatives by R. Skowronski*, G. Grabowski, J. Lewkowski, G. Descotes, L. Cottier and C. Neyret353
Synthesis of Pyrazoline and Isoxazoline Derivatives of Androstane Series by A. U. Siddiqui*, D. Ramesh, Y. Satyanarayana, M. Srinivas, and A. H. Siddiqui356
Asymmetric Inductive Synthesis of α-Aminoarylacetic Acids in the Presence of β-Cyclodextrin by W. Xu* and Y. Zhang360
A New Synthesis of Symmetric Piperazines Derivatives by J.-C. Lancelot, B. Leotis and M. Robba*363
Samarium Triiodide Catalyzed Dithioacetal and Dithioketal Formation by Y. Zhang*, Y. Yu and R. Lin365
A Convenient Synthesis of 7-Hydroxy-3-hydroxymethyl-4-phenyl-2-naphthoic Acid, Lactone Form by J. F. Payack* and D. R. Bender368
Corrigendum373
Synthesis of 9-Substituted Guanines. A Review by F. P. Clausen* and J. Juhl-Christensen373
Recent Progress in the Preparation and Synthetic Uses of the Reactions of 3H-Pyrazoles. A Review by T. Nagai* and M. Hamaguchi403
An Improved Preparation of (S)-N-(Boc)-Cyclohexylalaninal. The Moffat-Swern Oxidation of α-Aminoalcohols by D. J. Krysan*, A. R. Haight, J. E. Lallaman, D. C. Langridge, J. A. Menzia, B. A. Narayanan, R. J. Pariza, D. S. Reno, T. W. Rockway, T. L. Stuk and J. H. Tien437
Synthesis of 5,5'-Difluoro-bapta-am, a Useful in vivo Probe for Calcium Determination by P. E. Morris, Jr.445
Syntheses of Tetrasubstituted Cyclopentanes by K. Somekawa*, M. Nomura, S. Aoki, S. Noma, and T. Shimo449
An Efficient Synthesis of Boc-Aminoacetaldehyde and its Application to the Synthesis of N-(2-Boc-Aminoethyl)glycine Esters by K. L. Dueholm, M. Egholm and O. Buchardt*457
OPPI Briefs (J.-P. Anselme, Editor)463
Lipase-Catalyzed Transacylation Reactions in Azeotropic Distillation by G. Lin* and S.-H. Liu463
Thexyl- and Isopinocampheylhaloboranes as Stereoselective Reducing Agents by J. S. Cha*, S. J. Min, J. M. Kim, O. O. Kwon and M. K. Jeoung466
Bromoacetaldehyde and Iodoacetaldehyde by Ozonolysis of Allyl Bromide and Allyl Iodide by M. Jachak*, M. Mittelbach and H. Junek469
Synthesis of Spin-Labeled Triazenes by Z. Raikov*, V. Gadzheva, M. Koch and G. Kolar473
An Improved Large-Scale Preparation of 3,3',4,4'-Tetraaminodiphenyl Ether by A. R. Katritzky*, Z. Yang and D. J. Cundy478
Preparation and Reactions of Indolin-2(3H)-ones. A Review by G. M. Karp481
The Lateral Metalation of Isoxazoles. A Review by N. R. Natale* and Y. R. Mirzaei515
Preparation of Phenylglycolic Acids and Sodium p-(N,N-Dialkylamino)phenylglycolates by A. R. Katritzky*, B. Galuszka, S. Rachwal and D. Lynch557
Facile Large-scale Synthesis of 5-Alkyluracils by H. Koroniak*, A. Jankowski and M. Krasnowski563
Synthesis of 2-Aryl-4,5,6,7-tetrahydro-6,6-dimethyl-2H-benzo[d][1,2,3]triazol-4-ones by H. A. Hamid, A. Mousaad, M. Sayed and E. S. H. El Ashry*569
OPPI Briefs (J.-P. Anselme, Editor)577
An Improved Synthesis of 5-(3,4-Dimethoxyphenyl)-3-hydroxy-4-nitrocyclohexene by A. F. Ibañez*, A. R. Martinez and G. Y. Moltrasio Iglesias577
An Improved Procedure for the Preparation of 1,6-Dicarboxyhex-3-ene by P. T. Deota* and S. Abid579
A Facile Synthesis of bis(3-Aryl-3-oxo-1-propenyl)benzenes by J.-G. Shao, J.-F. Zhou, C.-Q. Liu and Q. Zhong*581
An Improved Synthesis of 2-Methallyloxyphenol by V. B. Deodhar*, V. S. Dalavoy, U. R. Nayak583
Synthesis of 1-Hydroxy-7-phenoxynaphthalene by A. R. Katritzky*, M. Balasubramanian and M. Siskin*587
Facile Synthesis of 2-Aryl-4H-3,1-benzoxazin-4-ones by D. V. Ramana* and E. Kantharaj588
Preparation of bis(2,2,2-Trifluoroethyl)selenide and telluride and of bis(2,2,2-Trifluoroethyl)diselenide and ditelluride by K. K. Bhasin*, V. Gupta, R. Khajuria and R. P. Sharma590
Synthesis of Pentafluorophenyl-4-(N-maleimidomethyl)cyclohexane-1-carboxylate (FMCC) by M. Adamczyk* and D. Johnson592
A Simple, Efficient Preparation of 1,1-bis(Trimethylsiloxy)-1,3-butadiene by G. S. Welmaker595
A One-Step Preparation and Hetero Diels-Alder Dimerization of 2-Phenylpropenal by T. Laitalainen*, P. Kuronen and A. Hesso597
A Simple and Practical Approach to Unsymmetrical Phenylureas by K. Ramadas* and N. Srinivasan600
Thiopheno[3,2][1]benzazepine, benzo[3,4]cyclohepta[2,1-b]thiophenes, thiazolo- [5,4-d][1]benzazepine and benzo[3,4]cyclohepta[2,1-d]thiazoles by V. Peesapati* and N. Lingaiah602
Progress in the Fischer Indole Reaction. A Review by D. L. Hughes607
Synthesis of Dimethyl 1,4-Dihydroxy-5,6,8-trimethoxynaphthalene-2,3-dicarboxylate, a Key Intermediate for Fredericamycin A by R. S. Mali* and P. G. Jagtap633
Synthesis of 2-O-Protected Glycerol Derivatives by J. M. Chong* and K. K. Sokoll639
Synthesis of Functionalized Acrylates by M. Curci, J.-L. Mieloszynski and D. Paquer*649
One-pot Synthesis of Novel 10-Aryl[1,2,4]triazolo[3',4':2,3][1,3,4]thiadiazepino[6,7-c]quinolin- 6(5H)-ones by A. Jayashree and M. Darbarwar*659
Synthesis of RL-252 Vanadyl Complex by M. W. Wilson and J. C. Hodges*665
Preparation of Optically Active New Mercapto Chiral Auxiliaries Derived from Camphor by D.-S. Lee, S.-M. Hung, M.-C. Lai, H.-Y. Chu and T.-K. Yang*673
OPPI Briefs (J.-P. Anselme, Editor)681
A New Method for the Synthesis of Diacyl Selenides byY. Zhang*, X. Jia and X. Zhou681
Synthesis of N-Methylated Quinolones by J. N. Domínguez* and J. Charris683
A Facile Synthesis of β-Damascone by P. A. Unnikrishnan687
A Simple Procedure for the Preparation of (Methyl- and Phenylthio)aryloxyacetonitriles by A. Jonczyk* and E.-H. Muttar690
A Convenient Method for the Synthesis of Flavanones by the Selective Oxidation of Flavan-4-ols with Hypervalent Iodine by O. V. Singh693
Chloroform-mediated DDQ Oxidation of N-Methoxyseptorinol, a Substance Isolated from the Fungus Septoria Nodorum Bark by M. Devys, M. Barbier*, J. F. Bousquet and A. Kollmann696
Synthesis of Carbenoxolone Analogs from Argentatin B by R. Martínez*, Ma. del Rosario Arellano-García, M. Martínez-Vazquéz and J. Gallegos A.698
Simple and Convenient Procedure for the Preparation of 1-Methyl-4-nitrobenzimidazole by V. Milata* and D. Ilavsk´703
Preparation of some 2,3-Dihydrobenzothiazole-2-carboxamides by H. P. Penner*, R. Garner and E. L. Scott, III705
An Improvement in the Synthesis of 1,2,4,9-Tetrahydrocarbazol-3-one by W. A. Boulanger* and V. Dolsen707
A Simple Preparation of 4-Amino-5-aryl-2H-imidazol-2-ones by M. Srivastava* and R. Lakhan708
Corrigendum711
Indexes713

An Organic Preparations and Procedures Inc. Publication OPPInc



[OPPI Home] [Submitting Manuscripts] [Subscription Information] [Notice to Agents] [Table of Contents, Author Indices, and Chemical Indices] [Computer Disks]

Copyright© 2008 by Organic Preparations and Procedures Inc. (OPP Inc.)