Organic Preparations and Procedures International
The New Journal for Organic Synthesis


Table of Contents Volume 26, 1994



Furanosesquiterpene Synthesis. An Updated Review by A. J. Allen, V. Vaillancourt and K. F. Albizati*1
Organotin Enolates in Organic Synthesis. A Review by I. Shibata* and A. Baba85
An Improved Method for the Preparation of 4-Aryl-2,6-diphenylpyrylium Perchlorates and their Reactions with Ammonia and Methylamine by T. Bak, D. Rasala and R. Gawinecki*101
OPPI Briefs (J.-P. Anselme, Editor)111
Preparation of O-[2-(2-Pyridyl)ethyl]- and O-[2-(Trimethylsilyl)ethyl]hydroxylamines by T. Henmi, T. Sakamoto, and Y. Kikugawa*111
A cis-1,2-Diamine from the Stereoselective Reduction of an α-Amino Enamine by S. V. D'Andrea, S. Zhao, S. A. Mizsak, J. P. Freeman and J. Szmuszkovicz*114
Aromatic Nitration of 2-Phenylhydrazones of 1,2-Dicarbonyl compounds Using Cerium(IV) Ammonium nitrate by H. V. Patel,* K. A. Vyas, S. P. Pandey and P. S. Fernandes118
A Straightforward Synthesis of O-Protected 3-Hydroxypropanal derivatives by D. Barbier, J.-P. Salvi, N. Walchshofer* and J. Paris121
Simple and Facile Oxidation of Aldehydes to Carboxylic Acids by B. R. Babu and K. K. Balasubramaniam*123
Oxidation of Flavanones with Lead Tetraacetate, Trimethyl Orthoformate and Perchloric Acid by M. S. Khanna125
Reagent-Controlled Asymmetric Diels-Alder reactions. A Review by T. Oh* and M. Reilly129
o-Hydroxyaryl Ketones in Organic Synthesis. A Review by A. Kotali* and P. A. Harris159
Asymmetric Reductions of Carbon-Nitrogen Double Bonds. A Review by Q.-C. Zhu and R. O. Hutchins* and M. K. Hutchins193
Convenient Synthests of 2,3,5-Triaryl-5-oxopentanoic Acids and of Their t-Butyl Esters by V. Dryanska* and A. Popovich237
An Efficient One-pot Conversion of α-Amino Acid Esters to γ-Amino-α,β-unsaturated Carboxylates by Z. Y. Wei and E. E. Knaus*243
β-Trifluoroacetylation of Lactams and Benzolactams by J.-P. Bouillon, C. Atès, C. Maliverney, Z. Janousek and H. G. Viehe*249
Recent Progress in the Use of Sulfonyl Radicals in Organic Synthesis. A Review by M. P. Bertrand257
The Synthesis and Reactions of Prismanes. Recent Developments by M. A. Forman* and W. P. Dailey*291
Facile and High-Yield Synthesis of New 4-Phosphoranylidene-4,5-Dihydropyrazol-5-ones by Reaction of Conjugated Azoalkenes with Phosphines by O. A. Attanasi*, P. Filippone and D. Giovagnoli321
A Simple and Efficient Preparation of Methoxymethyl Esters of Penicillins and Cephalosporins by J. Pankowski* and J. Winiarski327
A Simple Synthesis of the Heterocyclic S,S-Diphenylsulfiliminesby O. G. Vlasova, O. A. Rakitin* and L. I. Khmelnitski331
An Alternate Method for the Synthesis of Secondary Nitramines by Z. Daszkiewicz, A. Domanski and J. B. Kyziol*337
An Efficient, Large-Scale Synthesis of Idoxifene [()-1-{4-[2-(N-Pyrrolidino)ethoxy]pheny1}-1- (4-iodophenyl)-2-phenyl-1-butene] by R. McCague, G. A. Potter and M. Jarman*343
OPPI Briefs (J.-P. Anselme, Editor)347
Single-Step Synthesis of 2,3-Dihydro-2,2-dimethyl-1H-phenothiazin-4(10H)-ones by V. Gupta, A. Gupta, R. S. Rathore and R. R. Gupta*347
An Improved Synthesis of Thieno(2,3-b)quinolines via S-Oxides by S. P. Rajendran* and P. Shanmugam349
Oxidative Rearrangement of the Purine Ring Using Magnesium Monoperphthalate by A. Amer353
An Economical Preparation of 2-(2-Bromoethyl)-1,3-dioxane by J. B. Christensen* and A. Schluter 355
Synthesis of N-Phosphorylureas by Reaction of Phosphorylamides with N-Substituted Trichloroacetamides by J. Petrov*, I. Atanassova and V. Ognyanova357
Synthesis of 3-Acetoacetyl-7-methyl-2H,5H-pyrano[4,3-b]pyran-2,5-dione by B. Boutemeur-Kheddis, A. Bendaas, M. Hamdi* and R. Sakellariou and V. Sp&eagrave;ziale*360
A New Approach to Alkyl 2-oxoquinoline-3-acetates by Triphenylphosphine-induced Cyclization of Alkyl o-Formylmaleanilates by N. P. Argade, S. M. Babar and V. Balasubramaniyan* 362
Efficient Regioselective Alkylation of 2-Carboxamidopiperazine. Application to the Synthesis of the NMDA Competitive Antagonist (±)-CPP by P. Pevarello*, G. Scappi and M. Varasi366
Purification of 1,2-Dihydronaphthalene, an Important Intermediate in the Hydroprocessing of Naphthalene by M. D. Cagle, S. J. Firsan and E. J. Eisenbraun*370
The Preparation ofDelta2 Steroids. An Improved Procedure by P. Nowak, K. Blaszczyk and Z. Paryzek*374
An Improved Procedure for the Preparation of 1,3-Dithiane by H. K. Patney377
Preparation of Redox Derivatives of 3α-Hydroxy-5α-pregnane-11,20-dione by E. Pop*, M. E. Brewster, K. Prókai-Tátrai and N. Bodor378
Synthiesis of Pyrazolo(3,4-b)quinolines and their 1-Phenyl Derivatives by S. P. Rajendran,* M. Manonmani and S. Vijayalakshmi383
Oxidation of Amines by Dichlorodicyanoquinone (DDQ) with Trapping by Trimethylsilyl Cyanide by R. J. Sundberg*, M.-H. Theret and L. Wright386
Corrigendum391
Synthesis of Carcinogenic Oxygenated Derivatives of Benz[c]acridines. A Review by N. Motohashi*, M. Kawase and J. Emrani393
Synthesis of 4-(Nitrobenzyl- and Benzoyl)piperidine Derivatives by Nitration of Arylalkyl- piperidines by S. Ram*421
Synthesis of Imidazoquinolines and Imidazoisoquinolines from Azanaphthalene Carboxylic Acids by K. C. Langry*429
An Alternative Synthesis of Aryl and Heteroaryl Bromides from Activated Aryl Hydroxy Compounds by A. R. Katritzky*, J. Li, Christian V. Stevens and D. J. Ager439
A Convergent Synthesis of (±)-Sarcophytol-A Benzyl Ether by W. Li, J. Mao, Ying Li and Yulin Li*445
Reduction of Organic Compounds with Sodium Aluminum Hydride in Theoretical Amount by J. S. Cha* and H. C. Brown459
OPPI Briefs (J.-P. Anselme, Editor)465
Synthesis of Several N-Substituted Amino-2-pyridones by G. E. H. Elgemeie*, S. R. El-Ezbawy, H. A. Ali and A.-K. Mansour465
Improved Alkylation of Ethyl Acetoacetate and Diethyl Malonate by D. Barbry*, C. Faven and A. Ajana469
Improved Preparation of 4-Chloromethylphenyl Acetate by J. B. Christensen471
Synthesis and Competitive N- and O-Alkylation of 10-Methylpyrido[3,2-g]quinoline-4,6- dione by A. Mahamoud, J.-P. Galy and J. Barbe*473
A Convenient Preparation of 9H-Fluorene-9-acetic Acid by R. R. Goehring476
Regioselective Synthesis of10-Hydroxy-11-Methoxyaporphine (isoapocodeine) from (RS)-10,11-Dihydroxyaporphine (Apomorphine) by J. C. Kim* and W.-W. Park479
A Short Synthesis of Tridec-12-en-2-one, the Minor Constituent of the Bark of Litsea Elliptica (Lauraceae) by S. Mithran, A. S. Subbaraman and V. R. Mamdapur*482
Treatment of Conjugated Azoalkenes with N-Acyl-N'-tosylhydrazides. A Useful Entry to Asymmetric bis-Acylhydrazones by O. A. Attanasi*, S. Santeusanio and F. Serra-Zanetti*485
A Highly Stereoselective Transformation of β-Santalene To (E)-β-Santalol by P. A. Unnikrishnan488
A Superior Method for the Synthesis of 7a-Methyl-2,3,7,7a-tetrahydrinden-5(6H)-one by H. S. P. Rao* and K. S. Reddy491
A Simple and Short Synthesis of 2-(2'-Aminobenzylamino)benzyl Alcohol, a Constituent of Justicia Gendarussa Burm Leaves by V. P. Kamat* and J. K. Kirtany494
Addendum to Vol. 25, 595 (1993)498
Recent Developments in Tetrazole Chemistry. A Review by S. J. Wittenberger499
Synthesis of a S-4-Carboxyphenylalanine Derivative for Use in Peptide Synthesis by R. G. Franz, J. Weinstock*, R. R. Calvo, J. Samanen and N. Aiyar533
Preparation of Triols and Ethers related to Podophyllotoxin by M. A. Castro*, M. Gordaliza, J. M. M. del Corral and A. San Feliciano539
OPPI Briefs (J.-P. Anselme, Editor)549
A Convenient Synthesis of 3-(2-Methylpyridyl)acetic Acid Methyl Ester, a Pyrithiamine Intermediate by M. E. Ivanova, V. B. Kurteva and M. J. Lyapova*549
Convenient Synthesis of 2,3-Dihydroxy-2-methylpropanamide via 2,3-Epoxy-2-methylpropanamide by J. F. Pilichowski*, G. Mailhot and M. Bolte551
Synthesis of Alkyl Isothiocyanates from Primary Alkyl Amines using Dicyandiamide as a Dehydrosulfurizing Agent by T. Yamamoto*, A. Terada, T. Muramatsu and K. Ikeda555
An Improved Synthesis of 9-Chloro-1,8-p-menthadiene by T. S. Kaufman,R. P. Srivastava and R. D. Sindelar*557
5-Nitro-2-furyl Dimidoyl Disulfides by Iodine Oxidation of N-Aryl-5-nitro-2-thiofuramides by A. D. Mance and K. Jakopcic´*560
Resolution of 5-Vinyl-2-pyrrolidinone. A Practical Synthesis of (S)- and (R)-Vigabatrin by Z. Y. Wei and E. E. Knaus*567
Facile Synthesis of Pheromone of Dichocrocis Punctiferalis, a Serious Pest of Spices by S. A. Hassarajani, A. S. Subaraman and V. R. Mamdapur*571
Useful Syntheses of Pyrano- and Pyridoindoles by R. S. Mali* and A. Manekar-Tilve573
An Improved Synthesis of Nε-Fmoc-L-lysine and Nδ-Fmoc-L-ornithine by M. Henczi and D. F. Weaver*578
An Efficient and Convenient Procedure for Ester Hydrolysis by J. M. Khurana* and A. Sehgal580
Conversion of Aromatic Nitriles to Aldehydes by Sodium tris(Dialkylamino)aluminum Hydrides by J. S. Cha*, M. K. Jeoung, J. M. Kim, O. O. Kwon and J. C. Lee583
Synthesis and Reactions of Phosphinimines using Hydrazonoyl Halides by H. M. Hassaneen*, N. M. Elwan, H. A. Abdelhadi, M. T. Fouad and M. S. Algharib588
Oxidation of 3β-Acetoxy-5α-lanost-8-ene with Chromyl Chloride. The Preparation of 5a,8β-Lanost-9(11)-en-7-one Derivatives by K. Stalin´ski and Z. Paryzek*593
A Simple Procedure for the Preparation of 2-Phosphorylated Furanoses by C. Lamberth595
Synthesis of 1,3-Diamines by V. Constantinou-Kokotou* and G. Kokotos599
A Convenient Preparation of 4-Vinylphenylacetic Acid and Its Methyl Ester by S. W. Wright* and L. D. McClure602
Improved Synthesis of Fluoromethyl Phenyl Sulfone by D. P. Matthews*, R. A. Persichetti and J. R. McCarthy605
An Efficient One-step Synthesis of tert-Butyl Glycinate and tert-Butyl Sarcosinate by E. Cavelier, M. Rolland and J. Verducci*608
A Concise Synthesis of 8-Phenyloctadecanoic Acid by R. Sharma and V. E. Marquez*611
Corrigendum615
Recent Progress in the Synthesis of Avermectins and Milbemycins. A Review by T. A. Blizzard617
Synthesis of α,w-Alkanediols. A Review by S. A. Patwardhan645
OPPI Briefs (J.-P. Anselme, Editor)671
An Efficient Synthesis of (2R, 5R)- and (2R, 5R)-2-Methyl-5-hydroxyhexanoic Acid Lactones by M.-J. Wu* and J.-Y. Yeh671
Simplified Condition for Synthesis of Curcumin I and Other Curcuminoids by K. V. D. Babu and K. N. Rajasekharan* 674
A High-yield Synthesis of 3-Pentadecylpyridine by W. M. Stalick* and J. H. Murray677
An Improved Electrosynthetic Preparation of the Female Housefly Sex Phermone by F. A. Marquez, A. J. Zara, J. T. B. Ferreira* and L. O. de S. Bulhões*680
The Synthesis of 6-Propyl-2-selenouracil. The Selenium Analogue of the Anti-thyroid Drug PTU by W.-X. Hu* and F. S. Guziec, Jr.682
A Convenient Direct Preparation of 2-Cyanopyrimidine by W.-X. Hu*, R. Pankayatselvan and F. S. Guziec, Jr.685
Analogs of Tryptophan by E. Pop*, K. Prókai-Tátrai, M. E. Brewster and N. Bodor687
Product Selectivity in the Synthesis of Three Novel Phosphorus-Containing Heterocycles from Acyclic Precursors by Selection of Base Strength by C. C. Orji and A. G. Pinkus*691
Monosubstituted 2,2'-Bipyridines by M. Sprecher*, R. Breslow, O. Uziel and T. M. Link696
Synthesis of R-(+)-1,3-Dithiane 1-Oxide by P. C. B. Page*, R. D. Wilkes, and M. J. Witty702
Preparation of Metabolites of Imipramine and Phenytoin by M. Adamczyk*, J. R. Fishpaugh, J. C. Gebler and K. J. Heuser706
Indexes713

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