Organic Preparations and Procedures International
The New Journal for Organic Synthesis


Table of Contents Volume 30, 1998

Biomimetic and Synthetic Approaches to Marine Sponge Alkaloids Derived from bis-Pyridine Macrocycles. A Review by N. Matzanke, R. J. Gregg and S. M. Weinreb*1
2-Substituted Hexahydropyrimidines and their Tautomerismby K. N. Zelenin*, V. V. Alekseyev, I. V. Ukraintsev and I. V. Tselinsky53
Reduction of Organic Compounds with Thexyl-s-butoxyboraneby J. S. Cha*, S. W. Chang, J. M. Kim, O. O. Kwon, J. H. Chun, S. D. Cho and H. S. Lee63
Synthesis of (1R,3S)-3-Amino-1,2,2-trimethylcyclopentylmethanolby J. M. Blanco, O. Caamaño, F. Fernández, X. García-Mera* and J. E. Rodríguez71
Improved Synthesis of 7,7-Dimethyl-1,4-dioxo-2,3,4,5,6,7-hexahydroinden-2-yl-acetic and Propionic Acid from Citralby I. Kádas*, G. Árvai, G. Horváth79
OPPI Briefs (J.-P. Anselme, Editor)87
Microwave-promoted Synthesis of 1-Aryloxy-3-alkylamino-2-propanolsby B. Pchelka and J. Plenkiewicz*87
Facile Synthesis of p-(Dicyanomethylene)benzoquinonesby M. Nanasawa*, H. Takahashi and T. Kuwabara90
Synthesis and Cyclization of 1-N-(Nitroamidino)thioureas to 2,4-Diaminothiazoles by R. Bina, K. K. Thomas, G. C. Jenardonan and K. N. Rajasekharan*93
An Efficient Oxidation Arylsemicarbazides to the Azo Ureasby C. Wang, Y. Wang*, X. Wang, J. Li, H. Wang and S. Zhang97
A Simple, One-pot Procedure for the Preparation of Dopaminergic Alkylthioapomorphines by S. Berényi*, C. Csutorás, S. Gyulai and S. Makleit100
Regioselective Epoxide Ring-Opening to the Enantiomerically Pure å-Hydroxy Analogue of S-tert-Butyl Cysteine by F. Cavelier* and A.-M. Yim103
Improved Synthesis of o-Benzenedisulfonimide by F. A. Davis*, G. Sundarababu and H. Qi107
1-Alkylidene(arylidene)amino-2-aminoethanes and their Tautomerization to Imidazolidines by K. N. Zelenin* and I. V. Ukraintzev109
Improved Preparation of 5,6-Dichlorocyclohex-2-ene-1,4-dione by V. F. Ferreira and F. J. Schmitz*115
A Convenient Synthesis of (E)-(1-Propenylsulfonyl)benzene by L. M. Finkielsztein, E. N. Alesso, B. Lantaño, J. M. Aguirre and G. Y. M. Iglesias*117
The Asymmetric Pauson-Khand Reaction. A Reviewby S. T. Ingate and J. Marco-Contelles*121
The Development and Application of 1,3-Dithiane 1-Oxide Derivatives as Chiral Auxiliaries and Asymmetric Building Blocks for Organic Synthesis. A Reviewby S. M. Allin and P. C. B. Page*145
A Novel and Facile Synthesis of o-Acylbenzaldehydesby A. Kotali*, M. Papapetrou, V. Dimos and P. A. Harris177
An Efficient Procedure for the Preparation of Fmoc-Amino Acidsby S. P. Raillard*, A. D. Mann and T. A. Baer183
Cyclopropyl and Pyrazolyl Selenadiazolyl and Thiadiazolyl Sulfones and Their Reactivity by V. Padmavathi, R. P. Sumathi, M. V. R. Reddy and D. B. Reddy*187
Investigation of the Alkylation of Aromatic and Hydroaromatic Aldoximes with Halohydrins by E. GÜler*, N. Sen, A. Sirit, S. Kurbanov and R. Mirzaoglu195
Synthesis of Symmetrical and Unsymmetrical Disubstituted a-Pyrenylmethyl and a-Perylenylmethyl Malonate and Cyanoacetate Allyl Estersby A. R. Katritzky*, Z. Yang, and J. N. Lam and C. Nagel203
OPPI Briefs (J.-P. Anselme, Editor)211
A Novel Synthesis of 2-Amino Diarylketone Derivatives and of Polyfunctionally Substituted Quinolinesby F. Al-Omran*, A. A. El-Khair and M. H. Elnagdi*211
Preparation of Alumina-supported Dimethylammonium Chlorochromate (DMCC) and its Use in the Oxidation of Alcohols and Benzoinsby G.-S. Zhang*, Q.-Z. Shi, M.-F. Chen and K. Cai215
A Simple Regioselective Nuclear Bromination of Alkyl Phenyl Ethers by S. Yakabe, M. Hirano* and T. Morimoto*218
Synthesis of 3,6-Di-(tert-butyl)fluorene by Nickel(0) Catalyzed Coupling of Aryl Halidesby G. C. Paul* and J. J. Gajewski*222
Asymmetric Epoxidation of Unfunctionalized Olefins via Formation of Crystalline Cyclodextrin Complexesby H. Sakuraba* and Y. Tanaka226
Lithium Hypochlorite-Clorox as a Novel Oxidative Mixture for Methyl Ketones and Methyl Carbinolsby M. M. Madler, J. Klucik, P. S. Soell, C. W. Brown, S. Liu, K. D. Berlin*, D. M. Benbrook, P. J. Birckbichler and E. C. Nelson230
[3.3.1]Propellane-2,8-dione. Synthesis and Structureby I. D. Reingold*, G. Beckmann, A. M. Grannas, S. R. Brunette, B. D. Williams, S. Lovell and B. E. Kahr235
A Novel Method of Synthesis of Alkyl a-Cyanoacryloyl Glycolatesby X. Yang239
Recent Progress in the Synthesis and Reactions of Isothiochromans. A Reviewby Y.-C. Xu243
Syntheses of Avenaciolide and Related Bislactones. A Reviewby V. S. Mart�n*, C. M. Rodr�guez and T. Mart�n291
Borane-(N-substituted)benzotriazole Complexes and their Alkylation Reactions by A. R. Katritzky*, Y. Fang and S. A. Belyakov325
Convenient Preparation of 14-Hydro-5H-Tribenzo[a,d,f]cyclooctenesby T. Yamato*, N. Sakaue and K. Fujita331
Chemoselective Synthesis of Protected Polyamines and Facile Synthesis of Polyamine Derivatives Using O-Alkyl-O'-(N-succinimidyl) Carbonatesby M. Adamczyk*, J. R. Fishpaugh and K. J. Heuser339
OPPI Briefs (J.-P. Anselme, Editor)349
New Synthesis of Phenylthioglycolic Acids via Related Triazene Compounds by A. Disli and Y. Yildirir*349
A Simple Regioselective Synthesis of (R)-10-Hydroxyaporphine Directly from (R)-10,11-Dihydroxyaporphine [(R)-Apomorphine]by J. C. Kim*, S.-D. Bae, J.-A. Kim and S. K. Choi352
A New Synthesis of 6,7-Dichloro-dibenzo[c,f][2,7]-naphthyridines via Photocyclization by S. Vijayalakshmi and S. P. Rajendran*356
Synthesis of Disulfides by the Oxidative Coupling of Thiols with Calcium Hypochlorite and Silica Gel in Hexaneby M. Hirano*, S. Yakabe, N. Uraoka, and T. Morimoto*360
�ew Spiropyran-4-ylindolidine Derivatives from the Reaction of 2-Oxo-3-cyanomethyl- idene-2,3-dihydroindoles with Cyclohexanediones and Phenolsby F. Al-Omran*, I. EL-Ghamry and M. H. Elnagdi363
A Facile Synthesis of 5-Benzoylcytosine Derivativesby R. B. Toche, M. N. Jachak, T. S. Dalvi, R. W. Sabnis*, H. Junek , T. Kappe367
Applications of Trimethylsilyl Halides-Oxidants Combinations in Organic Synthesis. A Review by P. S. Vankar, M. V. R. Reddy and Y. D. Vankar*373
Photochemical Transformation of 2(5H)-Furanones. A Reviewby A. I. Hashem*, A. Senning and A.-S. S. Hamad401
A Rapid Williamson Synthesis Under Microwave Irradiation in Dry Mediumby D. Bogdal*, J. Pielichowski and K. Jaskot427
Facile Synthesis of 5-(Dihydroxyboryl)-2,4-bis(alkoxy)pyrimidines and N(1)-Substituted5-(Dihydroxyboryl)uracilsby H. Wojtowicz-Rajchel and K. Golankiewicz*433
Synthesis and Spectral Data of Some New N-Nitroso-N-Phenylhydroxylamine (Cupferron) Derivativesby A. T. Balaban*, R. E. Garfield, M. J. Lesko and W. A. Seitz439
OPPI Briefs (J.-P. Anselme, Editor)447
A Facile Synthesis of o-, m-, p-(Trimethylstannyl)benzyl Chlorides and Amines by A. B. Koldobsky, V. E. Vakhmistrov, O. S. Shilova, V. N. Kalinin*, K. A. Tehrani, N. De Kimpe447
Improved Preparation of Flurbiprofenby M. N. Deshmukh* and V. Lakshminarayana451
A Novel Route to 4-Arylidene-2-phenyl-5(4H)-oxazolonesby M. Kidwai* and R. Kumar453
Efficiency of the Vilsmeier-Haack Method in the Synthesis of p-Aminobenzaldehydes by R. Gawinecki,* S. Andrzejak and A. Puchala455
Improved Preparation of Surfactants Derived from Sucrose with Ultrasoundby J. Besson, C. Fayet, J. Gelas* and C. Lamazzi460
fn Efficient and Facile Procedure for Deprotection of 1,1-Diacetates Using Anhydrous Ferrous Sulfateby T.-S. Jin, Y.-R. Ma, Z. H. Zhang and T.-S. Li*463
A High Yielding Preparation of 2,2'-Bipyridine-1-oxideby F. W. Joachim Demnitz* and M. B. d�Heni467
Surface Mediated Synthesis of O-Phosphorothioatesby K. Ramadas*, N. Janarthanan and D. Meera Rani469
An Improved Preparation of S,S�-Dimethyl N-Cyanodithioiminocarbonate by L. K. Marble 473
New Syntheses of bis(Tetramethylene)fluoroformamidinium Hexafluorophosphate (BTFFH) and 1,3-Dimethyl-2-fluoro-4,5-dihydro-1H-imidazolium Hexafluorophosphate (DFIH). Utility in Peptide Coupling Reactionsby A. El-Faham477
Synthesis of Benzo[c][2,7]naphthyridines and 2,13-Diazabenzo[b]chrysene by C. F. Nutaitis*, M. L. Crawley and J. Obaza-Nutaitis481
Preparation of O-(3,3,8,10,10-Pentamethyl-1,2-dithia-5,8-diazacyclodecan-5-yl)ethyl O-Pivaloyloxymethyl Phenylphosphonateby N. Bodor*, P. Prokai-Tatrai, E. Koltai and L. Prokai485
Recent Progress in Solid Phase Heterocycle Syntheses. A Reviewby J. W. Corbett489
Recent Progress in the Synthesis, Properties and Reactions of Trisulfanes and their Oxides by E. L. Clennan* and K. L. Stensaas551
Corrigendum601
Recent Progress in the Synthesis of p-Quinones and p-Dihydroquinones through Oxidation of Phenol Derivatives. A Reviewby S. Akai and Y. Kita*603
Activation of Carboxylic Acids by Pyrocarbonates. Scope and Limitations. A Review by V. F. Pozdnev631
Substituted Glutaconic Acids and their Esters in Organic Synthesis. A Reviewby P. F. Vlad* and M. Z. Krimer657
OPPI Briefs (J.-P. Anselme, Editor)699
Highly Efficient Synthesis of Fatty Acid Dopamidesby Z. Czarnocki*, M. P. Matuszewska and I. Matuszewska699
Synthesis of 1,2- and 1,4-bis[a-(2,4,6-Trinitroanilino)acetamido]benzene as New Insensitive Explosives by B. P. Bandgar*, V. R. Damal and S. S. Pandit703
Mild and Selective Method for the Oxidative Cleavage of Acetals and Thioacetalsby B. P. Bandgar*, S. A. Kulkarni and J. N. Nigal706
The Synthesis of 3-Amino-2-Dialkylaminopyridinesby A. D. Dunn709
Trimethylammonium Chlorochromate (TMACC) Adsorbed on Alumina for Cleavage of Carbon-Nitrogen Double Bonds Under Non-Aqueous Conditionsby G.-S. Zhang*, D.-H. Yang and M.-F. Chen713
A Facile Synthesis of New 2-Phosphonobenzyloxy-1,3,2-benzoxaza(dioxa or diaza)- phospholesby J. Zhou* and R. Chen716

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