Organic Preparations and Procedures International
The New Journal for Organic Synthesis


Table of Contents Volume 32, 1-615 (2000)

Recent Advances in Clay-catalyzed Organic Transformations by M. D. Nikalje, P. Phukan and A. Sudalai*1
Improved and Expeditious Microwave Synthesis of Ethyl 1,3-Cyclohexadien-1-carboxylate by N. Tesson and S. Deshayes*41
A Novel Method for the Synthesis of 4H-Pyran-4-one Derivatives by A. Shahrisa*, R. Tabrizi and H. R. Ahsani47
An Improved Synthesis of Hypericin and Related Compounds by E. Gruszecka-Kowaliko* and L. H. Zalkow*57
Synthesis of 4-[4-(Bromomethyl)-2-oxazolyl]-2,6-bis(1,1dimethylethyl)phenol by J. R. Rizzo*, B. A. Anderson, L. J. Heinz, R. C. Hoying and J. A. Panetta63
Synthesis of 6-Chloromethyl Benzothiazolin-2-one and of 6-Chloromethyl Benzoxazolin-2-one by P. Carato, S. Yous and P. Depreux*69
Synthesis and Characterization of Isomeric 2,5-Dimethyl-6-phenyl-3-cyclohexene-1-methanol Analogs by G. M. Coppola*, R. Damon, M. Shapiro, K. Gunderson and M. Kolpak75
OPPI Briefs (J.-P. Anselme, Editor)81
Silica Gel Catalyzed Preparation of Cinnamic Acids under Microwave Irradiation by H. M. S. Kumar*, B. V. S. Reddy, P. T. Reddy, D. Srinivas and J. S. Yadav81
Synthesis and Characterization of N-Alkyl Hydroxyacetamides by L. S. Z. Rivera, L. Carrillo and T. Mancilla*84
An Improved Synthesis of 3-Cyano-4-fluorobenzyl Bromide by G. A. Cain88
A Novel Route to Thymol from m-Cresol by K. J. Divakar, V.V. Dhekne, B. D. Kulkarni, P. L. Joshi, and A. S. Rao*92
Synthesis of 4,6-Dinitroindole by V. V. Rozhkov*, A. M. Kuvshinov and S. A. Shevelev94
A Convenient Synthesis of N-Boc-4-formylpiperidine by G. A. Cain* and C. A. Teleha96
A Facile Method with Improved Yields in the Synthesis of 6-Aryl-pyrido[2',3':4,5]pyrimido[1,6-α]benzimidazoles by G. Suma, R. H. Bahekar and A. R. R. Rao*99
Synthesis of 3-Azabicyclo[3.1.0]Hexanes. A Review by G. R. Krow* and K. C. Cannon103
Hydrogen Peroxide and Air as Inexpensive Oxidants in Phase-Transfer Catalysis. A Review by S. Schrader and E. V. Dehmlow*123
Novel Stereoselective Synthesis of E-Aryl Aldoxime and Ketoxime O-Ethers by E. Abele,
R. Abele, J. Popelis and E. Lukevics*
153
A Convenient Synthesis of 2H-Pyran-2-ones and of 3- and 5- Bromo-2H-pyran-2-ones by S. I. Kotretsou and M. P. Georgiadis*161
Improved Procedure for the Large Scale Synthesis of 1,2,3,4,4α,9β-Hexahydrodibenzothiophene by J. C. DiCesare*, L. B. Thompson, R. J. Andersen and J. Nail169
Efficient and Facile Routes to Nitrones by A. R. Katritzky*, X. Cui, Q. Long, B. Yanga, A. L. Wilcox and Y.-K. Zhang175
OPPI Briefs (J.-P. Anselme, Editor)185
Rate Acceleration of the Baylis-Hillman Reaction using Crystalline Cyclodextrin Complexes by L. R. Reddy and K. R. Rao*185
Preparation and Reactivity of Certain Oxapolycyclic Systems by M. Sander and E. V. Dehmlow*189
An Efficient Oxidation of Long Chain Alkyl Methyl Sulfides to Sulfoxides by T. Yamamoto*, T. Hayakawa, M. Yoshino, S.-I. Hata, and Y. Hirayama192
Large Scale Preparation of Cell Permeable, Non-Phosphate-Containing Grb2 SH2 Domain Inhibitors by D.-G. Liu, Z.-J. Yao, Y. Gao and T. R. Burke, Jr.*197
A Convenient Synthesis of 3,5-Di-t-butylbromobenzene from Benzene by Z. Li,* Z. Zheng and H. Chen202
Amines via Nucleophilic 1,2-Addition to Ketimines. Construction of Nitrogen-Substituted Quaternary Carbon Atoms. A Review by A. G. Steinig* and D. M. Spero*205
Recent Advances in the Chemistry of Oximes by E. Ãbele and E. Lukevics*235
OPPI Briefs (J.-P. Anselme, Editor)265
Synthesis of (S)-(–)-1-[(9-Fluorenylmethoxycarbonyl)amino-5-carboxypentyl]-3-hydroxypyridinium Trifluroacetate by M. Adamczyk* and R. E. Reddy265
Microwave-assisted Synthesis of Triaryl Phosphates by A. D. Sagar*, N. A. Shinde and B. P. Bandgar*269
Simple and Practical Syntheses of Dibenzyl, Benzyl Ethyl and Benzyl Methyl Malonates by A. L. Silva, A. C.-Zúñiga and L. A. Maldonado*272
A One-pot Synthesis of Pyrazolo[3,4-β][1,4]oxazines by M. A. Raslan*, F. M. Abd El-Latif, H. H. Otto and K. U. Sadek276
A Rapid Method for the Cyclization of 2'-Hydroxychalcones into Flavones by M. Gupta, S. Paul, R. Gupta* and A. Loupy280
Rapid N-Alkylation of Carbazole, Phenothiazine and Acridone under Microwave Irradiation by X. Fan*, J. You, T. Jiao, G. Tan And X. Yu284
Esterification by Microwave Irradiation on Activated Carbon by X. Fan*, K. Yuan, C. Hao, N. Li, G. Tan and X. Yu287
Synthesis of 4-Borono-2-fluorophenylalanine by G. W. Kabalka*, N. K. Reddy, L. Wang and R. R. Malladi290
Preparation of bis-[Spirofluorene-9,4'-(1-aza-2-cyclopentene)[1,5-a]indoline-8'-yl] sulfone by E. O. Gogritchiani, H. Dürr* and Sh. A. Samsoniya293
An Optimized Preparation of 2,3-Dihydro-1-methyl-4-oxonaphthalene-1-carboxylic Acid
by A. G. L. Cascio, G. R. Labadie, M. G. Sierra and R. M. Cravero*
298
Facile and Efficient Synthesis of a-Aminophosphonate Derivatives of 1,3,4-Oxadiazole and 1,3,4-Thiadiazole by S.-M. Lu*302
Recent Progress on the Synthesis of Cyathane Type Diterpenes. A Review by D. L. Wright* and C. R. Whitehead307
Asymmetric Catalysis of Acyl Transfer by Lewis Acids and Nucleophiles. A Review by A. C. Spivey*, A. Maddaford and A. J. Redgrave331
Synthesis of Fluorescence Probes with a 2,6-Aminonaphthalene-Carbonyl Chromophore by C. Balo, F. Fernández, X. García-Mera and C. López*367
OPPI Briefs (J.-P. Anselme, Editor)373
Aromatic Hydroxylation by a New Cupric Nitrate-H2O2-Phosphate Buffer System by A. Nasreen and S. R. Adapa*373
A Convenient Preparation of Methyl 4-(2-Aminoethyl)benzoate by S. W. Wright376
An Efficient and Facile Preparation of 2,2',4,4'-Tetrabromodiphenylamine by X. Wang, C. Wang, X. Wang and Y. Wang*379
An Efficient and Scalable Synthesis of Methyl 3-Hydroxymethylbenzoate by M. H. Chen, J. G. Davidson, J. T. Freisler and J. Magano*381
Synthesis of 1-(p-Nitrobenzyl)azoles and 1-(p-Nitrobenzyl)benzazoles by C. Pardo, S. Graf, M. Ramos, E. Sesmilo and J. Elguero*385
Rapid and Selective Regeneration of Carbonyl Compounds from their Oximes under Mild, Neutral and Solvent-Free Conditions by B. P. Bandgar* and S. S. Makone391
A Convenient and Effective Method for the Synthesis of Tetraoxaquaterenes by R. Pajewski, R. Ostaszewski and J. Jurczak*394
An Improved Synthesis of 2,3-bis(Bromomethyl)-1,4-dimethoxybenzene by J. Eskildsen, T. Christensen, T. Reenberg, U. Larsen and J. B. Christensen*398
Preparation of Imidazo[2,1-β]thiazoles and Thiazolo[3,2-α]benzimidazoles Using S-Ethenylsulfilimines by K. Ikeda, S. Hata, Y. Tanaka and T. Yamamoto*401
Corrigendum407
An Overview of Synthetic Studies of Antibiotics from Myxobacteria by D. R. Williams*, J. J. Li*, and R. H. Hutchings409
Synthesis of New Furan-derived N-Substituted Aminomethanephosphonates by J. Lewkowski*, M. Rzezniczak and R. Skowronski453
An Improved Synthesis of ±18 Methyl Eicosanoic Acid by D. J. Cundy* and P. A. Gurr461
Reaction of N-[(Trimethylsilyl)methyl]carbodiimides with Bifunctional Nucleophiles by O. Tsuge*, T. Hatta, M. Shinozuka, H. Tashiro, H. Maeda, and A. Kakehi469
OPPI Briefs (J.-P. Anselme, Editor)481
New Method for Synthesis of (w-Chloroalkyl)pyrroles by B. Tu, C. Wang and J. Ma*481
Efficiency of the Urushibara Nickel Catalyzed Atmospheric Hydrogenation in the Synthesis of Aniline Derivatives by X. Liu, T. Jia, J. Chen, Z. Jiang*, H. Zhang and X. Huang*485
An Improved Synthesis of a-Methoxy-a-(trifluoromethyl)phenylacetic Acid (Mosher's Acid) by K. R. Buszek* and N. Sato488
Improved Synthesis of (R)- and (S)-b-Methyl-g-butyrolactone by K. R. Buszek* and N. Sato491
An Efficient Synthesis of Enantiopure 3-Chlorostyrene Oxide via Oxazaborolidine-
catalyzed Reduction by O. K. Choi and B. T. Cho*
493
A Novel Synthesis of 3-Substituted Imidazolidin-2-one-1-carbonyl Chlorides by W. Su, K. Huang and Y. Zhang*498
Improved Synthesis of 3,5,6-Trifluoropyridin-2,4-diol by E. Anselmi, J.-C. Blazejewski,
and C. Wakselman*
502
Recent Progress in Isolation, Bioactivity Evaluation and Total Synthesis of Diarylheptanoids. A Review by J. Zhu*, G. Islas-Gonzalez and M. Bois-Choussy505
A Continuous Procedure for Preparation of para Functionalized Aromatic Thiols Using Newman-Kwart Chemistry by S. Lin, B. Moon, K. T. Porter, C. A. Rossman, T. Zennie and J. Wemple*547
Dehydration of Cedrol to α-Cedrene Using Copper(II) Sulfate and other Acidic Salts by E. J. Eisenbraun*, K. W. Payne and J. S. Bymaster505
OPPI Briefs (J.-P. Anselme, Editor)563
Unexpected Dieckmann Condensation in the Synthesis of Methyl 6-(6-methoxy-2-
naphthyl)-6-oxohexanoate with an Arylcadmium Reagent by C. Balo, F. Fernández, X. García-Mera and C. Lopez*
563
Reductive Coupling of Ketones with Imines Promoted by the Titanium Tetrachloride/ Samarium System by Y. Ma and Y. Zhang*567
A Facile Synthesis of Aryl Isothiocyanates from Arylamines by Z. Li, X. Qian*, Z. Liu, Z. Li and G. Song571
Synthesis of 1,9-Diamidiniumacridine as a Potential Receptor for Phosphate Ester Recognition by R. P. Dixon*, J. S. Snyder, L. Bradley and J. Linnenbrink573
A Synthesis of (E)-ω-Carboxy-2-alkenoic Esters by R. A. Bunce* and D. M. Herron577
A Convenient Synthesis of cis-Urocanic Acid, an Endogenous Immunosuppressant by T. Mohammad* and H. Morrison*581
[2+2] Cycloadditions of Benzofuran-3(2H)-one Enamines with Dimethyl Acetylene-
dicarboxylate by N. Tunoglu and G. Okay*
584
Selective Catalytic Oxidation of Alcohols Using Hydrogen Peroxide by J. H. Wynne, C. T. Lloyd, D. R. Witsil, G. W. Mushrush and W. M. Stalick*588
A Lithiation Approach to 5-Substituted-1-benzenesulfonylpyrazoles by K. Turnbull* and A. P. Brower593
Silica Gel Promoted Solvent-Free Synthesis of Arylcarbinols and Ferrocenylcarbinols by W.-Y. Liu, Q-H. Xu and Y.-X. Ma*596
Synthesis of Thymyl Ethers and Esters Using Polymer-Supported Thymol Anion by P. P. Kumbhar*, U. R. Kapadi, D. G. Hundiwale, S. B. Attarde, P. M. Dewang and N. S. Pawar600
Indexes707

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